Faculty Works

Document Type

Article

Publication Date

11-28-2000

Abstract

The hybridization of DNA by sequential electrostatic and hydrogen-bonding immobilization of single-stranded complementary oligonucleotides at the air-water interface with cationic Langmuir monolayers is demonstrated. The complexation of the single-stranded DNA molecules with octadecylamine (ODA) Langmuir monolayers was followed in time by monitoring the pressure-area isotherms. A large (and slow) expansion of the ODA monolayer was observed during each stage of complexation in the following sequence: primary single-stranded DNA followed by complementary single-stranded DNA followed by the intercalator, ethidium bromide. Langmuir-Blodgett (LB) films of the ODA-DNA complex were formed on different substrates and characterized using quartz-crystal microgravimetry (QCM), Fourier transform infrared spectroscopy (FTIR), polarized-UV-vis and fluorescence spectroscopy, as well as thermal melting studies. These measurements clearly showed that hybridization of the complementary single-stranded DNA molecules had occurred at the air-water interface, leading to the characteristic double-helical structure. Furthermore, it was observed that the DNA molecules in the LB films were oriented parallel to the substrate withdrawal direction.

Publication Title

Langmuir

Start Page No.

9142

End Page No.

9146

ISSN

1520-5827

DOI

10.1021/la000753z

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